Bulletin of the Chemical Society of Japan p. 1977 - 1978 (1982)
Update date:2022-08-03
Topics:
Tanimoto, Shigeo
Oida, Tatsuo
Ikehira, Hideyuki
Okano, Masaya
Several 2-alkylthio- and 2-arylthio-1,3-dithiolanes were synthesized by the reaction of 2-ethoxy-1,3-dithiolane with aliphatic and aromatic thiols in the presence of ZnCl2.The lithiation of 2-alkylthio-1,3-dithiolanes with butyllithium in tetrahydrofuran followed by the addition of alkyl halides gave unsymmetrical dialkyl trithiocarbonates in moderately good yields.
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