Tetrahedron Letters p. 2763 - 2766 (1989)
Update date:2022-09-26
Topics:
King, J. F.
Rathore, Rajenda
In accord with mechanistic prediction a one-pot, two-stage, controlled chlorination-hydrolysis of HO(CH2)nSH gave the sultine when n=3 or 4, and the polymeric sulfinic ester when n=5 or 6; alkaline hydrolysis of either product yielded the corresponding sodium ω-hydroxy-1-alkanesulfinate.
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