Synthetic Communications p. 685 - 695 (2001)
Update date:2022-09-26
Topics:
Orelli
Blanco
Garcia
Hedrera
Perillo
A general procedure is described for the synthesis of unsymmetrically substituted N-aryl-N′-alkyl (or aryl) 1,n-alkanediamines 1 (n = 2-5) by reduction of ω-alkyl (or aryl) aminoalkanamides 2 with borane. Compounds 2 are easily obtained by aminolysis of the corresponding ω-haloalkanamides 3.
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