Journal of Organic Chemistry p. 2193 - 2195 (1983)
Update date:2022-08-05
Topics:
Whitesell, James K.
Minton, Mark A.
Felman, Steven W.
An efficient resolution of the title acid (1) by using (+)- and (-)-α-phenethylamine is described.The (+) acid was determined to be 1S by chemical correlation through (+)-cis-bicyclo<3.3.0>octan-2-one (3) with (+)-cis-bicyclo<3.3.0>oct-7-en-endo-2-ol (4) where the absolute configuration is known to be 1R.The 1R configuration for (-)-3 was consistent with the negative Cotton effect observed for this ketone.
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Doi:10.1021/ja01591a028
(1956)Doi:10.1055/s-0030-1260082
(2011)Doi:10.1063/1.481067
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(1931)
