Journal of Organic Chemistry p. 2122 - 2124 (1983)
Update date:2022-08-03
Topics:
Koreeda, Masato
Brown, Lindsey
Employing the Carroll reaction as a means of chirality transfer, a highly efficient, stereochemically controlled, and generally applicable synthesis of optically active 1,5-dimethylated acyclic chains has been developed; as an example, the synthesis of the optically active C-15 vitamin E side chains 7a and 7b from (+)-pulegone in 12.6percent and 11.7percent overall yields, respectively, is described.
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