Sudies on the Nactins: Total Synthesis of (+/-)-tert-Butyl 8-O-(tert-Butyldimethylsilyl)nonactate

DOI: 10.1021/jo00173a044

Source and publish data:

Journal of Organic Chemistry p. 5017 - 5022 (1983)

Update date:2022-08-03

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Authors:

Barrett, Anthony G. M.

Sheth, Hiten G.

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Article abstract of DOI:10.1021/jo00173a044

The title nonactic acid derivative (32) was prepared in racemic form from 2,3,5-tri-O-acetyl-γ-D-ribonolactone (17).Lactone 17 reacted with DBU to give 3-acetoxy-5-methylene-2,5-dihydrofuran-2-one (18), which on hydrogenation over Pd/CaCO3 stereoselective

Full text of DOI:10.1021/jo00173a044

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