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Palladium(II)-catalysed Acetalization of Terminal Olefins Bearing Electron-withdrawing Substituents with 1,3- and 1,2-Diols

DOI: 10.1039/c39830000848

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 848 - 849 (1983)

Update date:2022-08-04

Topics:

Authors:

Hosokawa, TakahiroHosokawa, Takahiro

Ohta, ToshiyukiOhta, Toshiyuki

Murahashi, Shun-IchiMurahashi, Shun-Ichi

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Article abstract of DOI:10.1039/c39830000848

Treatment of terminal olefins bearing electron-withdrawing groups with (R,R)-pentane-2,4-diol (2) in the presence of PdCl2-CuCl-O2 in 1,2-dimethoxyethane gives cyclic acetals such as (3) and (12b) via attack at the terminal carbon atom; the corresponding acetals are similarly formed from propane-1,3-diol (5) and ethylene glycol (8).

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