Transformations of benzothiadiphosphole system: General one-pot synthesis of 1,2,5-dithiaphosphepines and their precursor phosphanethiols

DOI: 10.1002/hc.20099

Source and publish data:

Heteroatom Chemistry p. 339 - 345 (2005)

Update date:2022-07-29

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Authors:

Baccolini, Graziano

Boga, Carla

Mazzacurati, Marzia

Monari, Magda

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Article abstract of DOI:10.1002/hc.20099

Treatment, at room temperature, of benzothiadiphosphole 1 with BrMg(CH ₂)₅MgBr gives intermediate A, which was allowed to stand for about 3 h at room temperature. The subsequent addition of RMgX to the reaction mixture and the final

Full text of DOI:10.1002/hc.20099

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