Tetrahedron Letters p. 909 - 912 (1995)
Update date:2022-09-26
Topics:
Kise, Naoki
Inakoshi, Naoto
Matsumura, Yoshihiro
Both diastereomers of 3-amino-2-hydroxyalkanoic acid derivatives were synthesized selectively by LDA-induced reaction of N-methoxycarbonyl-1-methoxyamines with O-protected N,N-dimethylglycolamides.The inversion of the diastereoselectivity was highly achieved by 1) selecting the O-protecting groups and 2) the addition of Ti(OPr-i)4.
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