A method for the chromatographic resolution of tetrahydropyran-2-ones

DOI: 10.1016/S0040-4020(01)80729-8

Source and publish data:

Tetrahedron p. 9939 - 9946 (1991)

Update date:2022-08-03

Topics:

Authors:

Ashworth

Belagali

Casson Casson

Marczak Marczak

Kocienski

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Article abstract of DOI:10.1016/S0040-4020(01)80729-8

The spirocyclic ortholactones prepared from certain tetrahydropyran-2-ones (valerolactones) and (1R)-1-phenylpropan-1,3-diol are readily separable by flash chromatography on silica gel. Hydrolysis of the resolved ortholactones then provides the pure homoc

Full text of DOI:10.1016/S0040-4020(01)80729-8

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