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REGIOSELECTIVE SYNTHESIS OF DIHYDROFURANS FROM 2,2-DIBROMO-1,3-DIKETONE AND OLEFIN USING COPPER

DOI: 10.1016/S0040-4039(01)81298-3

Source and publish data:

Tetrahedron Letters p. 2817 - 2820 (1984)

Update date:2022-08-05

Topics: Column chromatography   Yield   Olefin   Nucleophilic addition   Cyclization   TLC (thin-layer chromatography)   NMR (nuclear magnetic resonance)   Oxidative Addition   Reductive Elimination   Catalytic Cycle   Copper (Cu)   Reaction Optimization   Stoichiometry   Solvent Effect   Dihydrofurans   Regioselective synthesis   Inert atmosphere   Electrophilic bromination   GC-MS (Gas Chromatography-Mass Spectrometry)  

Authors:

Yoshida, Jun-ichiYoshida, Jun-ichi

Yano, ShinjiYano, Shinji

Ozawa, TadahiroOzawa, Tadahiro

Kawabata, NariyoshiKawabata, Nariyoshi

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Article abstract of DOI:10.1016/S0040-4039(01)81298-3

2,2-Dibromo-1,3-diketones reacted with copper powder and olefin to give 4,5-dihydrofuran derivatives in a highly regioselective fashion.

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Full text of DOI:10.1016/S0040-4039(01)81298-3

Products guided by the article

Product name:Cyclopropanecarboxylic acid, 1-acetyl-2-phenyl-, ethyl ester, cis-

Cas No:92898-25-4

92898-25-4

R&D Labs maybe for 92898-25-4

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