Tetrahedron Letters p. 4007 - 4010 (1984)
Update date:2022-08-05
Topics:
Fujisawa, Tamotsu
Iida, Sachio
Sato, Toshio
1-Chloro-2-methyl-N,N-tetramethylenepropenylamine was found to be an efficient condensation reagent for the regioselective coupling reaction of propargyl alcohols with Grignard reagents to give allenes in good yields with high chemo- and enantioselectivities.The utility of the reaction was demonstrated in the stereocontrolled synthesis of methyl (E)-2,4,5-tetradecatrienoate, the pheromone of the male dried bean beetle.
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