Journal of the Chemical Society. Chemical communications p. 1191 - 1192 (1984)
Update date:2022-08-05
Topics:
Holmes, Andrew B.
Raithby, Paul R.
Russell, Keith
Stern, Edward S.
Stubbs, Michael E.
Wellard, Nicholas K.
The azaspiro oxo-urethane (4), readily available from naphthalene, is reduced to the amino-alcohol (5) whose diacetate (6), the structure of which was determined by X-ray crystallography, undergoes acetate elimination in refluxing toluene to yield the N-acetylazaspiroundecene (7).
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(1984)
