Steroids p. 219 - 224 (1984)
Update date:2022-09-26
Topics:
Hylarides, Mark D.
Leon, Alberto A.
Mettler, Fred A.
The synthesis of the previously unknown 1-chloroestradiol (1), is reported.Addition of N-chlorosuccinimide/NaI in dioxane to 4-aminoestradiol 3-methyl ether (2), resulted in exclusive chlorination of the 1-position.Subsequent deamination and demethylation afforded 1 in good yields.
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