Journal of Organic Chemistry p. 3186 - 3188 (2009)
Update date:2022-08-11
Topics:
Marsh, Barrie J.
Carbery, David R.
A one-pot protocol for the formation of 2-nitrobenzenesulfonylhydrazide (NBSH) from commercial reagents and subsequent alkene reduction is presented. The transformation is operationally simple and generally efficient for effecting diimide alkene reductions. A range of 16 substrates have been reduced, highlighting the unique chemoselectivity of diimide as a reduction system.
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