Journal of the Chemical Society. Chemical communications p. 1266 - 1267 (1988)
Update date:2022-08-22
Topics:
Andrews, Mark A.
Klaeren, Stephen A.
Unprotected aldose sugars are smoothly decarbonylated by 1 equiv. of chlorotris(triphenylphosphine)rhodium in N-methylpyrrolidin-2-one at 130 deg C to give he next lower alditol and carbonylchloribis(triphenylphosphine)rhodium; ketose sugars undergo more complex dehydration-decarbonylation reactions.
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