Journal of Structural Chemistry p. 58 - 61 (1988)
Update date:2022-08-30
Topics:
Volkov, V. V.
Khikmatov, M.
Mirsaidov, U.
Gabuda, S. P.
Kozlova, S. G.
Usig the 1H, 11B, 139La NMR and relaxation MR methods, we have investigated the molecular dynamics in La(BH4)3 and its adduct with tetrahydrofuran La(BH3)3*3THF.We have observed phase transitions connected with the change in the nature of the internal rotation (reorientation) of the BH4- anions.We have determined the barrier to reorientation of the BH4- anions and the THF molecules in the investigated compounds, and we have shown that the change in the mobility of the THF molecule does not lead to a phase transition.
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