Tetrahedron Letters p. 9623 - 9626 (2000)
Update date:2022-08-10
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A synthesis of 13C, 15N labeled imidazoles was developed which allows the direct detection of a transient 2,5-endoperoxide at -100°C. The endoperoxide was thoroughly characterized by 1H, 13C, and 15N NMR. Upon warming, the endoperoxide decomposes via a series of transient intermediates to 13CO2 and 1,2-diphenyl-ethanediimine. (C) 2000 Elsevier Science Ltd.
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