Chemistry Letters p. 2101 - 2102 (1987)
Update date:2022-08-10
Topics:
Matsukawa, Mihaya
Tabuchi, Takanori
Inanaga, Junji
Yamaguchi, Masaru
Deoxygenation of epoxides to olefins was effected by an efficient electron transfer system of SmI2-THF-HMPA in the presence of N,N-dimethylaminoethanol (DMAE) or glutaric anhydride.This procedure, in combination with the SmI2-induced iodomethylation, afforded a new, rapid and mild one-pot carbonyl methylenation method.
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