Tetrahedron Letters p. 3623 - 3626 (1996)
Update date:2022-08-28
Topics:
Myers, Andrew G.
Yang, Bryant H.
Kopecky, David J.
Lithium amidotrihydroborate (LiH2NBH3, LAB) is a new and highly nucleophilic reducing agent that is easily prepared by deprotonation of the commercial reagent borane-ammonia complex (H2NBH3) with n-BuLi in tetrahydrofuran (THF) at 0°C. LAB is found to be a superior reagent for the transformation of tertiary amides into the corresponding primary alcohols.
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(1979)
