Tetrahedron p. 1259 - 1266 (1996)
Update date:2022-08-10
Topics:
Lozano, Jose I.
Barba, Fructuoso
The pathway for the electrochemical formation of 2-benzhydrylidene-4,4-diphenyl-[1,3]oxathiolan-5-one (2), in dichloromethane tetraethylammonium bromide on graphite cathode is proposed. It involves reaction between electrogenerated diphenylketene (3), 2-bromo-2,2-diphenylacetyl bromide (1) and sulfide anion. The latter is formed from H2S generated in the anodic compartment and electrogenerated bases.
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