Journal of the Chemical Society, Dalton Transactions p. 1151 - 1156 (1992)
Update date:2022-08-10
Topics:
Baghurst, David R.
Mingos, D. Michael P.
Using a thick-walled glass reaction vessel a number of transition-metal organometallic and co-ordination compounds have been synthesised using microwave dielectric super-heating effects.Super-heating by 40-60 deg C is maintained by controlling the pressure at 10 atm and results in a decrease in the reaction time required for conventional reflux reactions by a factor of ca. 102.Full details of the design of the apparatus, the modification of a conventional microwave oven and the electrical circuitry for the pressure control are provided.
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