Journal of Fluorine Chemistry p. 137 - 140 (1998)
Update date:2022-08-11
Topics:
Konno, Akinori
Shimojo, Moriyasu
Fuchigami, Toshio
Anodic fluorinations of ethyl isonicotinate (1) and related compounds have been attempted. Desired fluorinated product, 2-fluoroisonicotinate (2) was obtained in reasonable yield by direct anodic monofluorination of ethyl isonicotinate 1. The yield of 2 and the conversion of the electrochemical reaction could be improved by applying relatively lower anodic potential and by increasing the concentration of supporting electrolyte Et3N · 3HF.
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