Synthesis of [[2His13]Heptanoic acid via the desulfurization of methyl 3-chloro-5,6-dibromothieno[3,2,b]thiophe-2-carboxylase with Nickel-Aluminium alloy in NaOD-D2O solution

DOI: 10.1002/jlcr.2580341112

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 1087 - 1090 (1994)

Update date:2022-08-10

Topics:

Authors:

Tsuzuki Tsuzuki

Mukumoto

Tsukinoki

Mataka Mataka

Tashiro Tashiro

Yonemitsu

Nagano Nagano

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Article abstract of DOI:10.1002/jlcr.2580341112

[²H₁₃]Heptanoic acid was synthesized as its methyl ester (4) (deuterium content: 96%) with Ni-Al alloy in 10% NaOD-D₂O via the desulfurization of methyl 3-chloro-5,6-dibromothieno[3,2,b]thiophene-2-carboxy (3), which was derived from 4,5-dibromothiophene-2-carboaldehyde (1) in two steps.

Full text of DOI:10.1002/jlcr.2580341112

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Product name:HEPTANOIC-D13 ACID

Cas No:130348-93-5

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Zhejiang Haizhou Pharmaceutical Co., Ltd.

website:https://www.haizhoupharma.com/

Contact:+86-576-88221016

Address:No. 19, Donghai 5th Avenue, Yanhai Industrial Zone, Linhai, Zhejiang, China
Shanghai He Yang International Trading Co., Ltd.

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Ningbo Inno Pharmchem Co., Ltd.

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Hubei Lansun Biochemical Pharmaceutical Co., Ltd

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HUNAN CHEMAPI BIOLOGICAL TECHNOLOGY CO.,LTD.

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