Synthesis of [[2His13]Heptanoic acid via the desulfurization of methyl 3-chloro-5,6-dibromothieno[3,2,b]thiophe-2-carboxylase with Nickel-Aluminium alloy in NaOD-D2O solution

DOI: 10.1002/jlcr.2580341112

Source and publish data:

Journal of labelled compounds and radiopharmaceuticals p. 1087 - 1090 (1994)

Update date:2022-08-10

Topics:

Authors:

Tsuzuki Tsuzuki

Mukumoto

Tsukinoki

Mataka Mataka

Tashiro Tashiro

Yonemitsu

Nagano Nagano

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Article abstract of DOI:10.1002/jlcr.2580341112

[²H₁₃]Heptanoic acid was synthesized as its methyl ester (4) (deuterium content: 96%) with Ni-Al alloy in 10% NaOD-D₂O via the desulfurization of methyl 3-chloro-5,6-dibromothieno[3,2,b]thiophene-2-carboxy (3), which was derived from 4,5-dibromothiophene-2-carboaldehyde (1) in two steps.

Full text of DOI:10.1002/jlcr.2580341112

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