Bulletin of the Chemical Society of Japan p. 1097 - 1101 (1982)
Update date:2022-08-11
Topics:
Eiki, Toshio
Asai, Yoshio
Tagaki, Waichiro
The rates of the acid-catalyzed hydrolysis of phenyl phosphatosulfate (PPS) have been found to be highly dependent on the water content in the mixed solvent of acetonitrile-water.A remarkable rate acceleration was observed with a rate maximum near the 1:1 ratio of PPS and metal ion, and with a solvent with a low water content.Under such conditions, the site of the cleavage of the P-O-S linkage was observed to be predominantly the S-O bond.
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Doi:10.1021/ja408151h
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