Steroids p. 343 - 350 (1984)
Update date:2022-08-29
Topics:
Rao, P. Narasimha
Damodaran, K. M.
Starting from 11β-hydroxytestosterone, we achieved the synthesis of a strategic precursor, C-19(11) unsaturated 5α-androstane-3α,17β-diol 17-glucuronide (9a), for the preparation of 9α,11α-tritiated 5α-androstane-3α,17β-diol 17-glucuronide.We optimized the reaction conditions for catalytic reduction employing hydrogen and subsequent base hydrolysis followed by purification on Amberlite XAD-2 resin to obtain the saturated 5α-androstane-3α,17β-diol 17-glucuronide.
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