Journal of the Chemical Society. Perkin transactions I p. 883 - 893 (1996)
Update date:2022-08-31
Topics:
Johnson, A. Peter
Luke, Richard W. A.
Steele, Robert W.
Boa, Andrew N.
Bis(trimethylsilyl)formamide reacts with aldehydes in refluxing chloroform, or at room temperature with catalysis by trimethylsilyl trifluoromethanesulfonate, to give 1-acylamino-1-(trimethylsiloxy)alkanes; similar results are obtained with other bis(trimethylsilyl)amides, but surprisingly not with bis(trimethylsilyl)acetamide, and addition of bis(trimethylsilyl)formamide to ketones and acetals can also be accomplished using TMS triflate as catalyst.
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