Synthetic Photochemistry XXXVIII. The Photorearrangement of the Tropone Endoperoxide, 6,7-Dioxabicyclo-nona-3,8-dien-2-one

DOI: 10.1246/bcsj.60.3037

Source and publish data:

Bulletin of the Chemical Society of Japan p. 3037 - 3038 (1987)

Update date:2022-08-16

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Authors:

Mori, Akira

Takeshita, Hitoshi

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Article abstract of DOI:10.1246/bcsj.60.3037

The photolysis of 6,7-dioxabicyclo<3.2.2>nona-3,8-dien-2-one produced six photolysates, including a cage γ-lactone which belongs to the same type of product as was characterized in each case of the photolysis of the endoperoxides derived from 2-aryl- and 2,7-diaryltropones by Mukai et al.The new products identified were 2,7-dioxabicyclo-<3.2.2>nona-3,8-dien-6-one, a δ-lactone acetal, and 7-exo-formyl-3-oxabicyclo<4.1.0>hept-4-en-2-one, a δ lactone.

Full text of DOI:10.1246/bcsj.60.3037

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