Inorganic Chemistry p. 404 - 408 (1972)
Update date:2022-08-29
Topics:
Kifer, Edward W.
Van Dyke, Charles H.
Although the silicon-oxygen bond of siloxanes and alkoxysilanes is readily cleaved by phosphorus pentafluoride, the silicon-hydrogen bond of hydrosiloxanes can be easily fluorinated at low temperatures by this reagent thus providing a convenient source of fluorosiloxanes. The synthesis and characterization of FSiH2OSiH3, (FSiH2)2O, F(CH3)HSiOSiH2CH3, and [F(CH3)HSi]2O are described.
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