Synthetic Communications p. 1383 - 1386 (1991)
Update date:2022-08-11
Topics:
Behling
Farid
Medich
Scaros
Prunier
Weier
Khanna
The potent glucosidase inhibitor 1-deoxynojirimycin was synthesized from L-sorbose using a short synthesis and only one protecting group. The last step, which constituted the removal of an acetonide protecting group and an intramolecular reductive amination, was accomplished on an acidic ion-exchange resin. This provided a synthesis capable of being operated on a multi-kilogram scale.
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