Journal of Physical Chemistry p. 2009 - 2017 (1984)
Update date:2022-08-11
Topics:
Lewis, Nathan S.
Wrighton, Mark S.
Mediated outer-sphere redox processes have been examined at rotating disk Pt/<(PQ2+/+)n>surf electrodes.The <(PQ2+/+)n>surf is a redox polymer anchored to the surface and is formed from N,N'-bis<(trimethoxysilyl)propyl>-4,4'-bipyridinium, I.The polymer coverages for the electrodes selected for study are sufficiently great that Fe(phen)33+/2+, E0' = +1.03 V vs.SCE, shows no electrochemial response near its E0'.The mediated reduction of Fe(phen)33+ and a number of other outer-sphere oxidants is mass-transport limited when the Pt/<(PQ2+/+)n>surf electrode is held ca. 100 mV more negative than E0'<(PQ2+/+)n>surf = -0.45 v vs.SCE in CH3CN/0.1 M
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