Bulletin of the Chemical Society of Japan p. 3468 - 3470 (1991)
Update date:2022-08-11
Topics:
Kakiuchi, Kiyomi
Ue, Masaki
Yamaguchi, Bunji
Nishimoto, Atsushi
Tobe, Yoshito
Irradition of 3-methoxyphenol in the presence of 2 equiv. of AlBr3 in CH2Cl2 gave 4-methoxybicyclo<3.1.0>hex-3-en-2-one in a 38percent yield. 3-Methoxy-2-methylphenol also yielded the lumiketone rearrangement product.On the other hand, 3-methoxy-4-methyl-, 3-methoxy-5-methyl-, and 5-methoxy-2-methylphenol underwent transposition of the methyl group to give equilibrium mixtures of the three methoxycresoles.
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