Synthesis of 1,3,6,8-tetrabromophenanthrene via a stoichiometric Ullmann reaction

Article abstract of DOI:10.1080/00397910008087019

1,3,6,8-Tetrabromophenantherene (1) is prepared in four steps from 2,4,6-tribromobenzoic acid (4) in an overall yield of 12%. The key transformation used in the synthesis is a stoichiomteric Ullmann reaction.

Full text of DOI:10.1080/00397910008087019

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Synthetic Communications: An
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Synthesis of 1,3,6,8-
Tetrabromophenanthrene
via a Stoichiometric Ullmann
Reaction
John M. Farrar a , Monika Sienkowska a & Piotr
Kaszynski a
a Organic Materials Research Group Department of
Chemistry , Vanderbilt University , Nashville, TN,
37235
Published online: 04 Dec 2007.
To cite this article: John M. Farrar , Monika Sienkowska & Piotr Kaszynski (2000)
Synthesis of 1,3,6,8-Tetrabromophenanthrene via a Stoichiometric Ullmann Reaction,
Synthetic Communications: An International Journal for Rapid Communication of
Synthetic Organic Chemistry, 30:22, 4039-4045, DOI: 10.1080/00397910008087019
To link to this article: http://dx.doi.org/10.1080/00397910008087019
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