SIDE REACTIONS AND CADMIUM CATALYSED REMOVAL OF THE TRICHLOROETHOXYCARBONYL (TROC) PROTECTING GROUP.

DOI: 10.1016/S0040-4039(00)86799-4

Source and publish data:

Tetrahedron Letters p. 249 - 252 (1982)

Update date:2022-08-18

Topics:

Authors:

Hancock, G.

Galpin, I. J.

Morgan, B. A.

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Article abstract of DOI:10.1016/S0040-4039(00)86799-4

The Troc protecting group has been found to be unstable to the hydrogenolytic conditions used for removal of the benzyloxycarbonyl group; an improved method of removal employing cadmium dust in 50percent AcOH/DMF is described.

Full text of DOI:10.1016/S0040-4039(00)86799-4

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