Organic Letters p. 5752 - 5756 (2018)
Update date:2022-08-16
Topics:
Ganley, Jacob M.
Christensen, Melodie
Lam, Yu-Hong
Peng, Zhengwei
Angeles, Angie R.
Yeung, Charles S.
A metal-free, innate, and practical C-H formylation of nitrogen heterocycles using trioxane as a formyl equivalent is reported. This reaction provides a mild and robust method for modifying medicinally relevant heterocycles with an aldehyde handle. The use of an organic soluble oxidant, tetrabutylammonium persulfate, is critical in promoting the desired coupling.
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