Tetrahedron Letters p. 6123 - 6124 (1986)
Update date:2022-08-25
Topics:
Heisteeg, B. J. J. van de
Schat, G.
Tinga, M. A. G. M.
Akkerman, O. S.
Bickelhaupt, F.
The reaction of Me3SiCH(MgBr)2 with magnesium amalgam in diisopropyl ether furnished the di-Grignard reagent Me3SiCH(MgBr)2 in 70 percent yield.Derivatization with Me3SnCl gave Me3SiCH(SnMe3)2 (6,94percent).Witting type reaction occured readily with benzophenone (80percent), but the yield was low with cyclohexanone (13percent).
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(1991)
