Journal of Organometallic Chemistry p. 195 - 198 (1997)
Update date:2022-08-29
Topics:
Hughes, Andrew K.
Marsh, Sarah M.B.
Howard, Judith A.K.
Ford, Peter S.
The reaction of Ti(NMe2)4 with the amine functionalised cyclopentadiene C5H5CH2CH2CH2N(H)CMe3 gives the titanium cyclopentadienyl-amide complex [Ti{η5:σ1-(C5H4CH2CH2CH2NCMe3)}(NMe2)2] which reacts with aniline to generate the phenylimido bridged dimer [{Ti(η5-C5H4CH2CH2CH2N(H)CMe3)(NHPh)}2(μ-NPh)2] whose molecular structure has been determined by X-ray diffraction, revealing a slightly asymmetric Ti(μ,-NPh)2Ti core.
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