Journal of Fluorine Chemistry p. 349 - 358 (1988)
Update date:2022-08-16
Topics:
Modena, Silvana
Calini, Pierangelo
Gregorio, Guglielmo
Moggi, Giovanni
Liquid phase fluorination of diethyleneglycol dimethyl ether, tetraethyleneglycol dimethyl ether, 2<1,2-dichloro-1,2-difluoroethyl> tetrahydrofuran and 2<1,2-dichloro-1,2-difluoroethyl> dioxane 1,4 produce the corresponding perfluoroethers in 56, 43, 67 and 74 percent yields respectively.The by-products are partially fluorinated compounds and no fragmentation is observed.The simplicity of the reactions and method of preparation make this approach to fluorinated fluids and oils industrially attractive.
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