A novel synthesis of dialkyl 1-trimethylsilyloxy allyl phosphonates

Article abstract of DOI:10.1080/10426509608029638

Dialkyl 1-trimethylsilyloxy allylphosphonates (3a-3f) were synthesized by a one-pot reaction of trialkyl phosphite (1), carbonyl compounds (2) and trimethylchlorosilane. The procedure was carried out under very mild conditions and was very easy to conduct. The structures of (3) were confirmed by IR, ¹HNMR, ³¹P NMR and MS.

Full text of DOI:10.1080/10426509608029638

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Phosphorus, Sulfur, and Silicon and
the Related Elements
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A NOVEL SYNTHESIS OF DIALKYL
1-TRIMETHYLSILYLOXY ALLYL
PHOSPHONATES
Zhonghua Li a & Chuanfang Zhu a
a Department of Chemistry , Central China Normal
University , Wuhan, Hubei, 430070, China
Published online: 24 Sep 2006.
To cite this article: Zhonghua Li & Chuanfang Zhu (1996) A NOVEL SYNTHESIS OF DIALKYL 1-
TRIMETHYLSILYLOXY ALLYL PHOSPHONATES, Phosphorus, Sulfur, and Silicon and the Related
Elements, 108:1-4, 57-59, DOI: 10.1080/10426509608029638
To link to this article: http://dx.doi.org/10.1080/10426509608029638
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