A highly efficient and selective synthesis of lissoclinolide featuring hydrogen transfer hydrozirconation, trans-selective Pd-catalyzed cross coupling of alkenylzirconiums with 1,1-dibromoalkenes and Ag-catalyzed lactonization providing (Z)-γ-alkylidenebu

DOI: 10.1016/S0040-4039(98)02394-6

Source and publish data:

Tetrahedron Letters p. 431 - 434 (1999)

Update date:2022-08-29

Topics:

Authors:

Xu, Caiding

Negishi, Ei-ichi

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Article abstract of DOI:10.1016/S0040-4039(98)02394-6

An antibiotic lissoclinolide has been synthesized from propargyl alcohol in 9 steps and in 32% overall yield via (i) hydrogen transfer hydrozirconation of TBS-protected propargyl alcohol with i-BuZrCp₂Cl, (ii) Pd-catalyzed trans-selective cross

Full text of DOI:10.1016/S0040-4039(98)02394-6

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Product name:TERT-BUTYLDIMETHYL(2-PROPYNYLOXY)SILANE

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