An efficient inexpensive electrochemical preparation of Ruppert's reagent

DOI: 10.1016/S0040-4039(00)78453-X

Source and publish data:

Tetrahedron Letters p. 8623 - 8624 (1994)

Update date:2022-08-10

Topics:

Authors:

Aymard, Frederic

Nedelec, Jean-Yves

Perichon, Jacques

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Article abstract of DOI:10.1016/S0040-4039(00)78453-X

The electrochemical reduction of CF₃Br in N,N-dimethylformamide (DMF) in the presence of Me₃SiCl and a sacrificial aluminum anode provides Me₃SiCF₃ in ca 90% faradaic yields.

Full text of DOI:10.1016/S0040-4039(00)78453-X

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