PHENYL-PHENYL COUPLING IN TRIPHENYLANTIMONY CATALYSED BY PALLADIUM(0)

DOI: 10.1016/S0040-4020(01)85450-8

Source and publish data:

Tetrahedron p. 3111 - 3122 (1990)

Update date:2022-08-25

Topics:

Authors:

Barton, Derek H. R.

Khamsi, Jamal

Ozbalik, Nubar

Reibenspies, Joe

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Article abstract of DOI:10.1016/S0040-4020(01)85450-8

The Pd(0) induced coupling of phenyl groups in triphenylantimony to afford diphenyl and Sb(0) has been studied in a search for possible intermediates. Two complexes containing antimony and palladium have been isolated.Their structures have been determined by x-ray crystallography.Complex 1 is made up of triphenylantimony coordinated to palladium diacetate.It affords diphenyl nearly quantitatively on pyrolysis.Complex 2 contains a phenyl-palladium ?-bond as well as two coordinated triphenylantimony residues.

Full text of DOI:10.1016/S0040-4020(01)85450-8

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