Journal of the Chemical Society, Dalton Transactions p. 1965 - 1968 (1984)
Update date:2022-08-10
Topics:
Arifin, Zai
Filmore, Edward J.
Donaldson, John D.
Grimes, Susan M.
The Moessbauer parameters for the series of oxalatostannates(II) M2Sn(C2O4)2<*>xH2O are rationalised in terms of distorted square-pyramidal tin environments.The crystal structure of the malonato-complex K2Sn2a=11.233(2), b=18.776(2), c=8.171(1) Angstroem, β=90.15(1) deg, and Z=4; R=0.0277 for 5 805 reflections.Unlike the oxalate groups in the oxalato-complexes, the malonate moieties are bridging rather than chelating and the tin atoms are in trigonal rather than distorted four-pyramidal environments.Moessbauer data are reported for the malonate series of compounds M2Sn2
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