Glycine, N-[(dimethylamino)methylene]-, ethyl ester

Base Information

• Chemical Name: Glycine, N-[(dimethylamino)methylene]-, ethyl ester
• CAS No.: 30766-78-0
• Molecular Formula: C7H14N2O2
• Molecular Weight: 158.2
• Mol file: 30766-78-0.mol

Synonyms:N-(Dimethylaminomethylen)glycin-ethylester;(dimethylamino-methylenamino)-acetic acid ethyl ester;

Chemical Property of Glycine, N-[(dimethylamino)methylene]-, ethyl ester

Chemical Property:

• PSA: 41.90000
• LogP: 0.13940

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Glycine, N-[(dimethylamino)methylene]-, ethyl ester

There total 2 articles about Glycine, N-[(dimethylamino)methylene]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

tert-Butoxybis(dimethylamino)methane (5815-08-7) + GlyOEt*HCl (459-73-4) → ethyl N-<(dimethylamino)methylene>glycinate (30766-78-0) + dimethyl amine (124-40-3) + tert-butyl alcohol (75-65-0)

Guidance literature:

at 60 ℃; for 6h;

Reference yield: 59.0%

N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + GlyOEt*HCl (459-73-4) → ethyl N-<(dimethylamino)methylene>glycinate (30766-78-0) + dimethyl amine (124-40-3) + tert-butyl alcohol (75-65-0)

Guidance literature:

at 80 ℃; for 6h;

Reference yield:

ethyl N-<(dimethylamino)methylene>glycinate (30766-78-0) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) + Dimethyl-p-toluidine (99-97-8) + 2-chloro-7-fluoro-4-methyl-3,4-dihydrobenzo[e][1,4]diazepin-5-one (193693-31-1) → flumazenil (78755-81-4)

Guidance literature:

With n-butyllithium; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; n-heptane; dichloromethane;

upstream raw materials:

N,N-dimethyl-formamide dimethyl acetal

GlyOEt*HCl

tert-Butoxybis(dimethylamino)methane

Downstream raw materials:

flumazenil

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