ethyl 1-methyl-1-cyclopentanecarboxylate

Base Information

• Chemical Name: ethyl 1-methyl-1-cyclopentanecarboxylate
• CAS No.: 6553-72-6
• Molecular Formula: C₉H₁₆O₂
• Molecular Weight: 156.225
• Mol file: 6553-72-6.mol

Synonyms:ethyl 1-methyl-1-cyclopentanecarboxylate

Chemical Property of ethyl 1-methyl-1-cyclopentanecarboxylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 1-methyl-1-cyclopentanecarboxylate

There total 4 articles about ethyl 1-methyl-1-cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

cyclohexanol (108-93-0) + formic acid ethyl ester (109-94-4) → ethyl cyclohexanecarboxylate (3289-28-9) + ethyl 1-methyl-1-cyclopentanecarboxylate (6553-72-6) + 1-methylcyclopentanecarboxylic acid (5217-05-0) + Cyclohexanecarboxylic acid (98-89-5)

Guidance literature:

With sulfuric acid; at 45 ℃; for 1.5h; Product distribution; other temperature, different ratio of reactant/reagent;

Reference yield:

cyclohexane (110-82-7,25012-93-5) → ethyl cyclohexanecarboxylate (3289-28-9) + ethyl 1-methyl-1-cyclopentanecarboxylate (6553-72-6)

Guidance literature:

With sulfuric acid; under 58840.6 Torr; anschliessend mit Aethanol behandeln;

Reference yield:

ethanol (64-17-5) + cyclohexene (110-83-8) → ethyl cyclohexanecarboxylate (3289-28-9) + ethyl 1-methyl-1-cyclopentanecarboxylate (6553-72-6)

Guidance literature:

With sulfuric acid; under 58840.6 Torr;

upstream raw materials:

ethanol

carbon monoxide

cyclohexanol

formic acid ethyl ester

Downstream raw materials:

1-(4-methoxybenzyl)-N-(quinolin-8-yl)cyclopentanecarboxamide

1-methylcyclopentanecarboxylic acid

1-methylcyclopentanecarbonyl chloride

Refernces

• 1、 Ordyan, M. B.,Stepanyan, A. A.,Pirozhkov, S. D.,Manukyan, Sh. M.,Grigoryan, V. S.,Lapidus, A. L.. "ETHOXYCARBONYLATION OF CYCLOHEXANOL BY ETHYL FORMATE UNDER CONDITIONS OF CATALYSIS BY SULFURIC ACID". . p. 2290 - 2292. Retrieved 2007/10/02.