dicobalt octacarbonyl

Base Information

Chemical Name:dicobalt octacarbonyl
CAS No.:61091-28-9
Molecular Formula:C₈Co₂O₈
Molecular Weight:342.07
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicobalt octacarbonyl

Chemical Property:

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Technology Process of dicobalt octacarbonyl

There total 48 articles about dicobalt octacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: [di-μ-(ethoxycarbonyl-(methylene))-bis(tricarbonyl-cobalt) (Co-Co)]

: 201230-82-2
carbon monoxide

: 61091-28-9,15226-74-1,61117-58-6
dicobalt octacarbonyl

: 105-53-3
diethyl malonate

Guidance literature:: With ethanol; In hexane; High Pressure; soln. of Co2(CO)8 and EtOH placed in autoclave; pressurized (room temp.,50 bar CO); shaken (60 min); IR; gas chromy.;
DOI:10.1016/S1381-1169(03)00377-7

Reference yield: 80.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 16842-03-8,64519-62-6
hydridocobalt tetracarbonyl

: 67-56-1
methanol

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 107-31-3
Methyl formate

: 107-21-1
ethylene glycol

: 141-46-8
Glycolaldehyde

Guidance literature:: In dichloromethane; reaction of gaseous formaldehyde with excess of HCo(CO)4 in CH2Cl2 (0°C, 1 h), color of soln. turning brown; IR, 1H NMR;
DOI:10.1021/om00106a035

Reference yield: 65.0%

: cobalt(II) nitrate hexahydrate

: silver nitrate

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 128782-72-9
Ag⁽¹⁺⁾*{Co(CO)4}^(1-)=Ag{Co(CO)4}

: 7440-22-4
silver

Guidance literature:: With sodium dithionite; In ammonia; exclusion of air oxygen;; precipitation; washed with water, dried and washed with petrol ether; Ag dissolved in acetone; precipitated with water; dried in high vacuum over P2O5 (1h) protected from light;;