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13499-05-3

Basic Information
CAS No.: 13499-05-3
Name: Hafnium chloride(HfCl4), (T-4)-
Article Data: 11
Cas Database
Molecular Structure:
Molecular Structure of 13499-05-3 (Hafnium chloride(HfCl4), (T-4)-)
Formula: Cl4Hf
Molecular Weight: 320.302
Synonyms: Hafniumchloride (HfCl4) (6CI,8CI);Hafnium tetrachloride;Hafnium(IV) chloride;Tetrachlorohafnium;
EINECS: 236-826-5
Density: 1.89 g/cm3
Melting Point: 319 °C
Boiling Point: 319.0oC (sublimes)
Flash Point: N/A
Solubility: Soluble in water, methanol and acetone.
Appearance: white crystalline solid
Hazard Symbols: CorrosiveC
Risk Codes: 34
Safety: 26-36/37/39-45
Transport Information: UN 3260 8/PG 2
PSA: 0.00000
LogP: 2.75800
Synthetic route

(cyclopentadienyl)2hafnium dichloride

A

(η-cyclopentadienyl)hafnium trichloride

B

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
With CCl4; Cl2 Slow introduction of Cl2 (dried over H2SO4) through a gas inlet tube ending above the surface of stirred suspn. of HfCp2Cl2 and dry CCl4 (Ar, 20-23°C, ca. 30 min), occasional cooling of mixt. using ice/water bath.; Removal of Cl2 excess from mixt. with Ar, recovering of resulting materials by filtn. and washing (CCl4, CHCl3, petroleum ether), elem. anal.;A 55%
B n/a

2K(1+)*HfCl6(2-)=K2HfCl6

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) K2HfCl6 was decomposed at just below 500°C;

hafnium

7782-50-5

chlorine

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) sealing of Hf in vac. system, admitting of Cl2 (p(Cl2) = 200 mm), heating;

hafnium(IV) oxide

7719-09-7

thionyl chloride

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
In neat (no solvent, gas phase) thermal-sublimation column, Ar as carrier gas for SOCl2, heating (850°C, 20 min); drying the products over P2O5, elem. anal., product ratio depending on deposition temp.;
10025-67-9

disulfur dichloride

hafnium(IV) oxide

7440-44-0

pyrographite

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
1200 °C;;
1200 °C;;
56-23-5

tetrachloromethane

hafnium(IV) oxide

A

75-44-5

phosgene

B

127-18-4

1,1,2,2-tetrachloroethylene

C

124-38-9

carbon dioxide

D

7782-50-5

chlorine

E

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
In neat (no solvent) Kinetics; byproducts: O2; reaction bagins at 540K; mechanism discussed;;
In neat (no solvent) Kinetics; byproducts: O2; reaction bagins at 540K; mechanism discussed;;

hafnium carbide

7782-50-5

chlorine

13499-05-3

hafnium tetrachloride

hafnium(IV) oxide

7719-09-7

thionyl chloride

A

hafnium oxychloride

B

13499-05-3

hafnium tetrachloride

Conditions
ConditionsYield
With O2 In neat (no solvent, gas phase) thermal-sublimation column, dried O2-Ar mixture as carrier gas for SOCl2 (pressure: 13 kPa), heating (350 - 375°C, 15 - 120 min); drying the products over P2O5, elem. anal., product ratio depending on deposition temp., not separated;
1493-13-6

trifluorormethanesulfonic acid

13499-05-3

hafnium tetrachloride

hafnium tetrakis(trifluoromethanesulfonate)

Conditions
ConditionsYield
In not given Ar atmosphere; addn. of acid to Hf-salt, heating (50°C, 68 h); excess of acid removal, washing (petroleum ether), drying (0.5 mm Hg, 100°C, 8 h); elem. anal.;100%

SiMe2[NC(Ph)NH(tBu)]2

13499-05-3

hafnium tetrachloride

108-88-3

toluene

SiMe2[NC(Ph)NH(tBu)]2HfCl4·(C7H8)

Conditions
ConditionsYield
In tetrahydrofuran at 0 - 20℃; Inert atmosphere; Schlenk technique;100%
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    Product Name: HAFNIUM CHLORIDE CAS: 13499-05-3 MF: Cl4Hf MW: 320.3 EINECS: 236-826-5 Mol File: 13499-05-3.mol HAFNIUM CHLORIDE Structure HAFNIUM CHLORIDE Chemical Properties Melting point 432 °C (lit.) Boiling point 31

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Specification

The Hafnium chloride(HfCl4), (T-4)-, with the CAS registry number 13499-05-3 and EINECS registry number 236-826-5, has the systematic name of hafnium tetrachloride. It is a kind of white fine crystalline powder, and belongs to the following product categories: Straight chain Compounds; Crystal Grade Inorganics; HafniumMetal and Ceramic Science; Hafnium Salts; Metal and Ceramic Science; Salts. And the molecular formula of the chemical is Cl4Hf.

The characteristics of Hafnium chloride(HfCl4), (T-4)- are as followings: (1)H-Bond Donor 0; (2)H-Bond Acceptor 0; (3)Rotatable Bond Count 0; (4)Exact Mass 321.81901; (5)MonoIsotopic Mass 319.82196; (6)Topological Polar Surface Area 0; (7)Heavy Atom Count 5; (8)Formal Charge 0; (9)Complexity 19.1 ; (10)Isotope Atom Count 0; (11)Defined Atom StereoCenter Count 0; (12)Undefined Atom StereoCenter Count 0; (13)Defined Bond StereoCenter Count 0; (14)Undefined Bond StereoCenter Count 0; (15)Covalently-Bonded Unit Count 1.

You should be cautious while dealing with this chemical. It causes burns. Therefore, you had better take the following instructions: Wear suitable protective clothing, gloves and eye/face protection, and if in case of contacting with eyes, rinse immediately with plenty of water and seek medical advice. What's more, if you feel unwell, seek medical advice immediately (show label where possible).

Addtionally, the following datas could be converted into the molecular structure:
(1)SMILES: [Cl-].[Cl-].[Cl-].[Cl-].[Hf]
(2)InChI: InChI=1/4ClH.Hf/h4*1H;/p-4
(3)InChIKey: NOUGWYUJLNDWEG-XBHQNQODAZ