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373-52-4

Basic Information
CAS No.: 373-52-4
Name: Methane, bromofluoro-(6CI,7CI,8CI,9CI)
Article Data: 8
Cas Database
Molecular Structure:
Molecular Structure of 373-52-4 (Methane, bromofluoro-(6CI,7CI,8CI,9CI))
Formula: CH2BrF
Molecular Weight: 112.929
Synonyms: Fluorobromomethane;
EINECS: 206-770-6
Density: 1.773 g/cm3
Melting Point: N/A
Boiling Point: 19 °C at 760 mmHg
Flash Point: None
Solubility: N/A
Appearance: Clear colourless to light yellow liquid
Hazard Symbols: ToxicT
Risk Codes: 36/37/38
Safety: 26-36/37/39
Transport Information: N/A
PSA: 0.00000
LogP: 1.30830
Synthetic route
1868-53-7

dibromofluoromethane

373-52-4

bromofluoromethane

Conditions
ConditionsYield
53.1%
With sodium amalgam In water; isopropyl alcohol50%
1868-53-7

dibromofluoromethane

A

593-53-3

Methyl fluoride

B

373-52-4

bromofluoromethane

Conditions
ConditionsYield
With ethanol; zinc
353-59-3

halon-1211

A

1511-62-2

bromodifluoromethane

B

75-10-5

Difluoromethane

C

373-52-4

bromofluoromethane

D

75-09-2

dichloromethane

E

75-45-6

Chlorodifluoromethane

F

74-95-3

1,1-dibromomethane

Conditions
ConditionsYield
With hydrogen In gas at 400 - 900℃; under 760 Torr; Rate constant; Product distribution; Mechanism; other reagents; Ea;
34557-54-5

methane

75-63-8

Bromotrifluoromethane

A

74-83-9

methyl bromide

B

593-60-2

Vinyl bromide

C

373-52-4

bromofluoromethane

D

75-46-7

trifluoromethan

E

75-38-7

Vinylidene fluoride

F

74-95-3

1,1-dibromomethane

Conditions
ConditionsYield
Mn exchaged zeolite ZSM-5 at 599.85℃; Product distribution; other catalysts, temp.;
13126-91-5

silver(I) monofluoroacetate

373-52-4

bromofluoromethane

Conditions
ConditionsYield
With bromine at 20 - 80℃; for 1h; Bromination;
With bromine at 50 - 120℃; for 6h; Sealed tube;1.4 g
silver-fluoroacetate

silver-fluoroacetate

373-52-4

bromofluoromethane

Conditions
ConditionsYield
With bromine
1868-53-7

dibromofluoromethane

64-17-5

ethanol

zinc

zinc

A

593-53-3

Methyl fluoride

B

373-52-4

bromofluoromethane

397864-40-3

6α,9α-difluoro-17α-(furan-2-yl)carbonyloxy-11β-hydroxy-16α-methyl-3-oxoandrosta-1,4-diene-17β-carbothioic acid

373-52-4

bromofluoromethane

397864-44-7

fluticasone furoate

Conditions
ConditionsYield
In butanone at 0 - 22℃;99.3%
With sodium hydrogencarbonate In N,N-dimethyl-formamide at -20℃;88%
Stage #1: 6α,9α-difluoro-17α-(furan-2-yl)carbonyloxy-11β-hydroxy-16α-methyl-3-oxoandrosta-1,4-diene-17β-carbothioic acid With sodium carbonate In N,N-dimethyl-formamide at -15 - -5℃; for 0.25h;
Stage #2: bromofluoromethane In N,N-dimethyl-formamide at -15 - -5℃; for 3.3h;
79.08%
373-52-4

bromofluoromethane

4-bromobutyl thiophene-2-carboxylate

C10H13FO2S

Conditions
ConditionsYield
With nickel(II) bromide dimethoxyethane; C9H11N3; tetra-(n-butyl)ammonium iodide; potassium carbonate; 2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane In 1-methyl-pyrrolidin-2-one at 60℃; for 24h; Inert atmosphere; Sealed tube; Glovebox;97%
373-52-4

bromofluoromethane

1356857-65-2

tert-butyl 3-(tert-butoxycarbonyl)aminomethyl-3-methyl-4-(hydroxyimino) pyrrolidine-1-carboxylate

1356857-68-5

tert-butyl 3-(tert-butoxycarbonyl)aminomethyl-3-methyl-4-(fluoromethoxyimino)pyrrolidine-1-carboxylate

Conditions
ConditionsYield
With sodium hydroxide In water; toluene at 20℃; Cooling;96.1%
Downstream Products
80474-14-2
28523-86-6
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Specification

The Methane, bromofluoro-(6CI,7CI,8CI,9CI) is an organic compound with the formula CH2BrF. The IUPAC name of this chemical is bromo(fluoro)methane. With the CAS registry number 373-52-4, it is also named as Bromofluoromethane. The product's category is Fluoro-containing Compounds. Besides, it is clear colourless to light yellow liquid, which is an important reagent in the manufacture of intermediates, pharmaceuticals and other chemicals.

Physical properties about Methane, bromofluoro-(6CI,7CI,8CI,9CI) are: (1)ACD/LogP: 0.94; (2)ACD/LogD (pH 5.5): 0.94; (3)ACD/LogD (pH 7.4): 0.94; (4)ACD/BCF (pH 5.5): 3.03; (5)ACD/BCF (pH 7.4): 3.03; (6)ACD/KOC (pH 5.5): 76.99; (7)ACD/KOC (pH 7.4): 76.99; (8)Index of Refraction: 1.375; (9)Molar Refractivity: 14.57 cm3; (10)Molar Volume: 63.6 cm3; (11)Polarizability: 5.77×10-24cm3; (12)Surface Tension: 19.3 dyne/cm; (13)Density: 1.773 g/cm3; (14)Enthalpy of Vaporization: 25.49 kJ/mol; (15)Boiling Point: 19 °C at 760 mmHg; (16)Vapour Pressure: 940 mmHg at 25°C.

Uses of Methane, bromofluoro-(6CI,7CI,8CI,9CI): it can be used to produce 2-acetylamino-2-fluoromethyl-malonic acid diethyl ester at temperature of -35 °C. This reaction is a kind of Alkylation. It will need reagent (Et2N)3P=NMe and solvent CH2Cl2. The yield is about 49.9%.

When you are using this chemical, please be cautious about it as the following:
This chemical is irritating to eyes, respiratory system and skin. When you are using it, wear suitable gloves and eye/face protection. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: BrCF
(2)InChI: InChI=1/CH2BrF/c2-1-3/h1H2
(3)InChIKey: LHMHCLYDBQOYTO-UHFFFAOYAQ
(4)Std. InChI: InChI=1S/CH2BrF/c2-1-3/h1H2
(5)Std. InChIKey: LHMHCLYDBQOYTO-UHFFFAOYSA-N