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4-Hydroxybutyl acrylate
Cas No: 2478-10-6
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
4-Hydroxybutyl acrylate
Cas No: 2478-10-6
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1,4-Butyleneglycol acrylate
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Cas No: 2478-10-6
USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
2-Propenoic acid,4-hydroxybutyl ester 2478-10-6
Cas No: 2478-10-6
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier
2-Propenoic acid,4-hydroxybutyl ester CAS 2478-10-6
Cas No: 2478-10-6
No Data 1 Kilogram 50000 Kilogram/Day Wuhan Monad Medicine Tech Co.,LTD Contact Supplier
2-Propenoic acid,4-hydroxybutyl ester
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4-Hydroxybutyl acrylate CAS:2478-10-6 from fandachem
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4-Hydroxybutyl acrylate
Cas No: 2478-10-6
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4-Hydroxybutyl acrylate
Cas No: 2478-10-6
USD $ 1.0-1.0 / Gram 1 Gram 1 Metric Ton/Day PRIME MOLECULAR CO.,LIMITED Contact Supplier

2478-10-6 Usage

Chemical Properties

clear liquid
InChI:InChI=1/C7H12O3/c1-2-7(9)10-6-4-3-5-8/h2,8H,1,3-6H2

2478-10-6 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (275573)  4-Hydroxybutylacrylate  90%, contains 50 ppm monomethyl ether hydroquinone as inhibitor, 300 ppm hydroquinone as inhibitor 2478-10-6 275573-25G 386.10CNY Detail
Alfa Aesar (L11097)  4-Hydroxybutyl acrylate, 95%, stab. with ca 500ppm 4-methoxyphenol    2478-10-6 25g 961.0CNY Detail
Alfa Aesar (L11097)  4-Hydroxybutyl acrylate, 95%, stab. with ca 500ppm 4-methoxyphenol    2478-10-6 5g 295.0CNY Detail

2478-10-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Hydroxybutyl acrylate

1.2 Other means of identification

Product number -
Other names 4-Hydroxybutyl2-propenoate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Intermediates
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:2478-10-6 SDS

2478-10-6Synthetic route

Butane-1,4-diol
110-63-4

Butane-1,4-diol

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With 10H-phenothiazine; dioctyltin(IV) oxide In cyclohexane at 85℃; for 10h; Concentration; Reagent/catalyst;98.3%
vinyloxybutyl acrylate

vinyloxybutyl acrylate

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 40℃; under 225.023 Torr; for 1h;91%
Butane-1,4-diol
110-63-4

Butane-1,4-diol

acrylic acid
79-10-7

acrylic acid

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With toluene-4-sulfonic acid; 4-methoxy-phenol; hydroquinone In cyclohexane at 60 - 120℃; Temperature;82.5%
toluene-4-sulfonic acid
With 10H-phenothiazine; sulfuric acid In cyclohexane at 85℃; for 12h;
With toluene-4-sulfonic acid; hydroquinone
4-((4-methoxybenzyl)oxy)butyl acrylate

4-((4-methoxybenzyl)oxy)butyl acrylate

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With ammonium peroxydisulfate; 9-(2-mesityl)-10-methylacridinium perchlorate In dichloromethane; water at 20 - 30℃; for 3h; Irradiation; Green chemistry;45%
Butane-1,4-diol
110-63-4

Butane-1,4-diol

acetylene
74-86-2

acetylene

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With acetic acid; tetracarbonyl nickel
1,4-Butanediol diacrylate
1070-70-8

1,4-Butanediol diacrylate

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With phosphate buffer; carboxylesterase from Brevibacterium linens IFO 12171 In water at 30℃; pH=7.0; Enzyme kinetics; Hydrolysis; Enzymatic reaction;
Butane-1,4-diol
110-63-4

Butane-1,4-diol

acrolein
107-02-8

acrolein

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
Stage #1: acrolein With tert-butylhypochlorite In tetrachloromethane at 30℃; for 3.33333h;
Stage #2: Butane-1,4-diol In tetrachloromethane at 25℃; for 1.5h;
Butane-1,4-diol
110-63-4

Butane-1,4-diol

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

A

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

B

1,4-Butanediol diacrylate
1070-70-8

1,4-Butanediol diacrylate

Conditions
ConditionsYield
With Novozyme 435 In tert-Amyl alcohol at 50℃; for 120h; Inert atmosphere; Molecular sieve; Enzymatic reaction;
With Novozyme 435 In 2-methyl-2-butanol at 50℃; for 24h; Enzymatic reaction;
Butane-1,4-diol
110-63-4

Butane-1,4-diol

acryloyl chloride
814-68-6

acryloyl chloride

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; Inert atmosphere; Cooling with ice;
With triethylamine
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

4-(chlorocarbonyloxy)butyl prop-2-enoate
185756-32-5

4-(chlorocarbonyloxy)butyl prop-2-enoate

Conditions
ConditionsYield
With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In dichloromethane at -5 - 20℃; for 22.5h; Inert atmosphere;100%
With N,N-diethylaniline In ethyl acetate at 5℃; for 3h;273 g
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

4-tert-butyldimethylsilyloxy-1-butyl acrylate
756480-45-2

4-tert-butyldimethylsilyloxy-1-butyl acrylate

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 20℃; for 24h;98%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

acetylacetone
123-54-6

acetylacetone

C19H32O8
1108203-14-0

C19H32O8

Conditions
ConditionsYield
With N,N,N',N'-tetramethylguanidine at 40℃; for 4h; Michael Condensation;98%
Methyltrichlorosilane
75-79-6

Methyltrichlorosilane

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

C22H36O9Si

C22H36O9Si

Conditions
ConditionsYield
With hydroquinone at 100℃; for 2.5h; Large scale;92.1%
succinic acid anhydride
108-30-5

succinic acid anhydride

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-(4-(acryloyloxy)butoxy)-4-oxobutanoic acid
136153-20-3

4-(4-(acryloyloxy)butoxy)-4-oxobutanoic acid

Conditions
ConditionsYield
With dmap In dichloromethane at 25℃; for 48h; Inert atmosphere; Darkness;92%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

C32H52O12Si

C32H52O12Si

Conditions
ConditionsYield
With tetrachlorosilane; hydroquinone at 100℃; for 2.5h; Large scale;90.1%
oenanthic acid
111-14-8

oenanthic acid

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-(heptanoyloxy)butyl acrylate
1370407-32-1

4-(heptanoyloxy)butyl acrylate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 12h; Cooling with ice;90%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-<7-<4-<(dimethylthexylsilyl)oxy>phenyl>heptylidene>benzoic acid
162380-33-8

4-<7-<4-<(dimethylthexylsilyl)oxy>phenyl>heptylidene>benzoic acid

(acrylyloxy)-1,4-tetramethylene 4-<7-<4-<(dimethylthexylsilyl)oxy>phenyl>heptylidene>benzoate
162380-34-9

(acrylyloxy)-1,4-tetramethylene 4-<7-<4-<(dimethylthexylsilyl)oxy>phenyl>heptylidene>benzoate

Conditions
ConditionsYield
With bis-2-propyl carbonate; 4-(dimethylamino)pyridinium tosylate In dichloromethane for 25h;88.2%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

cyanoacetic acid
372-09-8

cyanoacetic acid

C10H13NO4
45162-96-7

C10H13NO4

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; for 2h;88%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

2-[(4-methoxybenzyl)oxy]-3-nitropyridine
350848-02-1

2-[(4-methoxybenzyl)oxy]-3-nitropyridine

4-((4-methoxybenzyl)oxy)butyl acrylate

4-((4-methoxybenzyl)oxy)butyl acrylate

Conditions
ConditionsYield
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 20℃; for 0.0833333h;87%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

benzaldehyde
100-52-7

benzaldehyde

(4-hydroxybutyl)-2-(α-hydroxybenzyl)acrylate
130977-36-5

(4-hydroxybutyl)-2-(α-hydroxybenzyl)acrylate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane for 72h; Ambient temperature;85%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

(2-dimethylamino-1-(4-morpholinophenyl)-2-(4-carboxyphenylmethyl)butan-1-one)

(2-dimethylamino-1-(4-morpholinophenyl)-2-(4-carboxyphenylmethyl)butan-1-one)

C31H40N2O6

C31H40N2O6

Conditions
ConditionsYield
Stage #1: 4-hydroxybutyl acrylate; (2-dimethylamino-1-(4-morpholinophenyl)-2-(4-carboxyphenylmethyl)butan-1-one) With thionyl chloride In dichloromethane; N,N-dimethyl-formamide for 2h;
Stage #2: With triethylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 1h;
83%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

rhodamine B
81-88-9

rhodamine B

Cl(1-)*C35H41N2O5(1+)

Cl(1-)*C35H41N2O5(1+)

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 24h;80.2%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

(4-(tert-butyl)benzyl)(trifluoromethyl)sulfane

(4-(tert-butyl)benzyl)(trifluoromethyl)sulfane

(E)-2-(3-(4-hydroxybutoxy)-3-oxoprop-1-en-1-yl)-4-(tert-butyl)benzyl trifluoromethyl sulfane

(E)-2-(3-(4-hydroxybutoxy)-3-oxoprop-1-en-1-yl)-4-(tert-butyl)benzyl trifluoromethyl sulfane

Conditions
ConditionsYield
With [2,2]bipyridinyl; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; copper diacetate at 80℃; for 12h; Sealed tube;80%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-<(2R)-2-cyano-7-<4-<<<4'-(pentyloxy)-4-biphenyl>carbonyl>oxy>phenyl>heptylidene>benzoic acid
151608-77-4

4-<(2R)-2-cyano-7-<4-<<<4'-(pentyloxy)-4-biphenyl>carbonyl>oxy>phenyl>heptylidene>benzoic acid

(acrylyloxy)-1,4-tetramethylene-4-<(2R)-2-cyano-7-<4-<<<4'-(pentyloxy)-4-biphenyl>carbonyl>oxy>phenyl>heptylidene>benzoate

(acrylyloxy)-1,4-tetramethylene-4-<(2R)-2-cyano-7-<4-<<<4'-(pentyloxy)-4-biphenyl>carbonyl>oxy>phenyl>heptylidene>benzoate

Conditions
ConditionsYield
With bis-2-propyl carbonate; 4-(dimethylamino)pyridinium tosylate In dichloromethane for 24h;78.5%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4‑((4,5‑diphenyl)‑1H‑imidazol‑2‑yl)benzoic acid
5496-35-5

4‑((4,5‑diphenyl)‑1H‑imidazol‑2‑yl)benzoic acid

C29H26N2O4

C29H26N2O4

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 10.5h; Cooling with ice;76.44%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

cyclopenta-1,3-diene
542-92-7

cyclopenta-1,3-diene

4-hydroxybutyl-bicyclo[2.2.1]hept-5-ene-2-carboxylate

4-hydroxybutyl-bicyclo[2.2.1]hept-5-ene-2-carboxylate

Conditions
ConditionsYield
Stage #1: 4-hydroxybutyl acrylate With dmap; 1-ClCOOCH2CH2O-2-MeO-4-HOCOCH2-5-BzNHCH2-C6H2; dacarbazine In pyridine; N,N-dimethyl-formamide at 0 - 20℃; for 25h; Esterification;
Stage #2: cyclopenta-1,3-diene In tetrahydrofuran at 60℃; for 15h; Cycloaddition; Diels-Alder reaction;
Stage #3: With penicillin G acylase In methanol at 37℃; for 48h; pH=7.0; Substitution; Product release;
75%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

2,5-bis-(4-butoxybenzoyloxy)-benzoic acid
205689-93-6

2,5-bis-(4-butoxybenzoyloxy)-benzoic acid

2,5-bis-(4-butoxybenzoyloxy)benzoic acid 4-acryloyloxybutyl ester

2,5-bis-(4-butoxybenzoyloxy)benzoic acid 4-acryloyloxybutyl ester

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; Inert atmosphere;75%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

N-((2-chloro-1,1,2,2-tetrafluoroethyl)sulfinyl)-2-methyl-2-phenylpropionamide

N-((2-chloro-1,1,2,2-tetrafluoroethyl)sulfinyl)-2-methyl-2-phenylpropionamide

1-[2-(4-hydroxylbutoxyl)-2-oxoethyl]-4,4-dimethyl-1,4-dihydroisoquinolin-3(2H)-one

1-[2-(4-hydroxylbutoxyl)-2-oxoethyl]-4,4-dimethyl-1,4-dihydroisoquinolin-3(2H)-one

Conditions
ConditionsYield
With silver(I) acetate; palladium diacetate; sodium carbonate at 80℃; Schlenk technique; Sealed tube;74%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

1-benzylsulfanyl-4-methyl-benzene
5023-60-9

1-benzylsulfanyl-4-methyl-benzene

C21H24O3S

C21H24O3S

Conditions
ConditionsYield
With silver tetrafluoroborate; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; copper diacetate at 80℃; for 12h;72%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

N-((2-chloro-1,1,2,2-tetrafluoroethyl)sulfinyl)pivalamide

N-((2-chloro-1,1,2,2-tetrafluoroethyl)sulfinyl)pivalamide

4-hydroxybutyl 2-(4,4-dimethyl-5-oxopyrrolidin-2-yl)acetate

4-hydroxybutyl 2-(4,4-dimethyl-5-oxopyrrolidin-2-yl)acetate

Conditions
ConditionsYield
With silver(I) acetate; palladium diacetate; sodium carbonate at 120℃; Schlenk technique;70%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-hydroxy-benzaldehyde
123-08-0

4-hydroxy-benzaldehyde

C14H16O4

C14H16O4

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 10.5h; Cooling with ice;67%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

C45H56O6

C45H56O6

4-[2-(3,4,5-trihexyloxyphenyl)vinyl]benzoic acid 4'-(4-acryloyloxybutoxy)biphenyl-4-ylester

4-[2-(3,4,5-trihexyloxyphenyl)vinyl]benzoic acid 4'-(4-acryloyloxybutoxy)biphenyl-4-ylester

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 70℃; for 12h; Mitsunobu Displacement; Inert atmosphere;66%
2-bromomethylfuran
4437-18-7

2-bromomethylfuran

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

C14H18O6

C14H18O6

Conditions
ConditionsYield
Stage #1: 4-hydroxybutyl acrylate With carbon dioxide; N,N,N',N'-tetramethylguanidine In N,N-dimethyl-formamide at 30℃; under 7500.75 Torr; for 1h; Autoclave;
Stage #2: 2-bromomethylfuran With carbon dioxide In N,N-dimethyl-formamide at 30℃; under 22502.3 Torr; for 24h; Autoclave;
65%
isobornyl methacrylate
16868-12-5

isobornyl methacrylate

styrene
292638-84-7

styrene

2-hydroxypropyl methacrylate
923-26-2

2-hydroxypropyl methacrylate

4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

methacrylic acid methyl ester
80-62-6

methacrylic acid methyl ester

2-methyl-butyl acrylate
97-88-1

2-methyl-butyl acrylate

poly(n-bytyl methacrylate-co-4-hydroxybutyl acrylate-co-2-hydroxypropyl methacrylate-co-isobornyl methacrylate-co-methyl methacrylate-co-styrene)

poly(n-bytyl methacrylate-co-4-hydroxybutyl acrylate-co-2-hydroxypropyl methacrylate-co-isobornyl methacrylate-co-methyl methacrylate-co-styrene)

Conditions
ConditionsYield
Stage #1: isobornyl methacrylate; styrene; 2-hydroxypropyl methacrylate; 4-hydroxybutyl acrylate; methacrylic acid methyl ester; 2-methyl-butyl acrylate In acetic acid butyl ester; ethyl acetate at 110℃; for 5h;
Stage #2: With tert-butyl peroxyacetate; azobis(2-cyanobutane) In acetic acid butyl ester; ethyl acetate for 6.5h; Heating / reflux;
60.4%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

2-(Hydroxy-p-tolyl-methyl)-acrylic acid 4-hydroxy-butyl ester

2-(Hydroxy-p-tolyl-methyl)-acrylic acid 4-hydroxy-butyl ester

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane for 144h; Ambient temperature;60%
4-hydroxybutyl acrylate
2478-10-6

4-hydroxybutyl acrylate

(R)-1,1'-Bi-2-naphthol
18531-94-7

(R)-1,1'-Bi-2-naphthol

Acrylic acid 4-(2'-hydroxy-[1,1']binaphthalenyl-2-yloxy)-butyl ester

Acrylic acid 4-(2'-hydroxy-[1,1']binaphthalenyl-2-yloxy)-butyl ester

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate Ambient temperature;60%

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