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poly(methacrylic acid)
diphenylolpropane diglycidyl ether
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
Stage #1: poly(methacrylic acid); diphenylolpropane diglycidyl ether With 2,6-di-tert-butyl-4-methyl-phenol at 105 - 108℃; for 2.25h; Stage #2: With N,N'-dimethylbenzylamine at 105℃; for 21h; Stage #3: With triethyleneglycol dimethacrylate |
BPA
2,3-Epoxypropyl methacrylate
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
With N,N'-dimethylbenzylamine at 70℃; for 6h; Inert atmosphere; Green chemistry; |
methacrylic acid methyl ester
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium cyanide; 2,4-dimethyl-6-tert-butylphenol / 2 h / 70 - 80 °C / Green chemistry 2: N,N'-dimethylbenzylamine / 6 h / 70 °C / Inert atmosphere; Green chemistry View Scheme |
BPA
methacrylic acid methyl ester
glycerol
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
Stage #1: BPA; glycerol With potassium carbonate; Diethyl carbonate at 110℃; for 18h; Stage #2: methacrylic acid methyl ester In dimethyl sulfoxide at 110℃; |
3-[4-[1-[4-(2,3-dihydroxypropoxy)phenyl]-1-methylethyl]phenoxy]propane-1,2-diol
methacrylic acid methyl ester
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
With potassium carbonate at 90℃; for 18h; Temperature; |
2-Isocyanatoethyl methacrylate
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
2,2-bis-4(3-methacryloxy-2-hydroxypropoxy)phenylpropane diurethane dimethacrylate
Conditions | Yield |
---|---|
In tetrahydrofuran at 40℃; for 24h; | 95% |
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
poly[2-methacrylic acid 2-hydroxy-3-[4-(1-{4-[2-hydroxy-3-(methacryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-propyl ester], photocured stereolithography
Conditions | Yield |
---|---|
With Camphorquinone UV-irradiation; |
triethyleneglycol dimethacrylate
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
With water; sodium dodecyl-sulfate; Camphorquinone Product distribution / selectivity; Irradiation with visible light; | |
With water; sodium dodecyl-sulfate; N,N-bis-(2-hydroxyethyl)-P-toluidine; dibenzoyl peroxide Product distribution / selectivity; Irradiation with light; | |
With sodium dodecyl-sulfate; N,N-bis-(2-hydroxyethyl)-P-toluidine; dibenzoyl peroxide Product distribution / selectivity; Irradiation with light; |
triethyleneglycol dimethacrylate
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
With ethyl p-dimethyaminolbenzoate; (1S,4R)-1,7,7-trimethylbicyclo[2.2.1]heptane-2,3-dione at 40℃; for 13h; Reactivity; Under yellow light; |
triethyleneglycol dimethacrylate
(1-methylethylidene)bis[4,1-phenyleneoxy(2-hydroxy-3,1-propanediyl)] bismethacrylate
Conditions | Yield |
---|---|
With ethyl p-dimethyaminolbenzoate; (1S,4R)-1,7,7-trimethylbicyclo[2.2.1]heptane-2,3-dione at 40℃; for 13h; Reactivity; Under yellow light; |
Molecular Formula: C29H36O8
Molar mass: 512.59 g/mol
EINECS: 216-367-7
Density: 1.161 g/cm3
Flash Point: 214.6 °C
Index of Refraction: 1.542
Boiling Point: 670.3 °C at 760 mmHg
Vapour Pressure: 7E-19 mmHg at 25°C
Product categories of Boron trifluoride dihydrate (1565-94-2): Acrylic Monomers;Bisphenol Acrylics
Structure of Boron trifluoride dihydrate (1565-94-2):
XLogP3-AA: 5.1
H-Bond Donor: 2
H-Bond Acceptor: 8
Systematic Name: [2-Hydroxy-3-[4-[1-[4-[2-hydroxy-3-(2-methylprop-2-enoyloxy)propoxy]phenyl]-1-methyl-ethyl]phenoxy]propyl] 2-methylprop-2-enoate
SMILES: O=C(OCC(O)COc1ccc(cc1)C(c2ccc(OCC(O)COC(=O)\C(=C)C)cc2)(C)C)\C(=C)C
InChI: InChI=1/C29H36O8/c1-19(2)27(32)36-17-23(30)15-34-25-11-7-21(8-12-25)29(5,6)22-9-13-26(14-10-22)35-16-24(31)18-37-28(33)20(3)4/h7-14,23-24,30-31H,1,3,15-18H2,2,4-6H3
InChIKey: AMFGWXWBFGVCKG-UHFFFAOYAI
Std. InChI: InChI=1S/C29H36O8/c1-19(2)27(32)36-17-23(30)15-34-25-11-7-21(8-12-25)29(5,6)22-9-13-26(14-10-22)35-16-24(31)18-37-28(33)20(3)4/h7-14,23-24,30-31H,1,3,15-18H2,2,4-6H3
Std. InChIKey: AMFGWXWBFGVCKG-UHFFFAOYSA-N
1. | mic-sat 800 µLg/plate | TOLED5 Toxicology Letters. (Elsevier Scientific Publishing Co., P.O. Box 211, Amsterdam, Netherlands) V.1- 1977- 31 (Suppl),(1986),214. | ||
2. | dni-hmn-hla 80 µmol/L | MUREAV Mutation Research. 368 (1996),181. |
Reported in EPA TSCA Inventory.
Mutation data reported. When heated to decomposition it emits acrid smoke and irritating vapors.
Hazard Codes: Xi
Risk Statements:
41: Risk of serious damage to eyes
Safety Statements:
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
Boron trifluoride dihydrate (1565-94-2) also can be called Silux ; Adaptic ; Panavia opaque ; Bis-gma ; 2,2-Propanediylbis(4,1-phenyleneoxy-2-hydroxy-3,1-propanediyl) bis(2-methylacrylate) ;and 2-propenoic acid, 2-methyl-, (1-methylethylidene)bis(4,1-phenyleneoxy-2-hydroxy-3,1-propanediyl) ester .